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ball mill swl serial 530 a01

Powders were milled in planetaryball mill(P5, Fritch) using acetone medium for 10-12 hrs. Milled powder were dried and calcined at temperature of 1100 C for 4hrs. Sintering was done by two step process first heated to 1300 for 4 hrs and then heated to 1500 C for 6hrs. X-ray powder diffraction was done using Bruker (D8, advance)

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